I'd love a DIY mass spectrometer or liquid chromatograph for biohacking!
https://bryanhanson.github.io/FOSS4Spectroscopy
You can try building that one. It's a DIY raman spectrometer.
I'm still holding out hope someone will make an open source FT-IR design. I actually need one for a project I'm working on, and I'd prefer not to shell out thousands of dollars for a used machine.